Acetone → 2,2-Dimethyl-5-(1-methylethylidene)-1,3-dioxane-4,6-dione

反応式

[CH3:1][C:2]1([CH3:10])[O:7][C:6](=[O:8])[CH2:5][C:4](=[O:9])[O:3]1.[CH3:11][C:12]([CH3:14])=O>>[CH3:1][C:2]1([CH3:10])[O:7][C:6](=[O:8])[C:5](=[C:12]([CH3:14])[CH3:11])[C:4](=[O:9])[O:3]1

参加物

反応物 2

HCID 180Acetone

HCID 162492,2-Dimethyl-1,3-dioxane-4,6-dione

生成物 1

HCID 752182,2-Dimethyl-5-(1-methylethylidene)-1,3-dioxane-4,6-dione

実験手順

This compound was prepared by using procedures analogous to those described for the synthesis of Example 120, Step 1 starting from acetone and 2,2-dimethyl-1,3-dioxane-4,6-dione.

後処理

customThis compound was prepared

出典と根拠

ORDレコード: ord-2a03ce76c00f4dd7a6122fb8d8d09a66
出典データセット: uspto-grants-2013_07
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08481732B2

反応ノート

読み込み中…