Potassium Cyanide → 2-(2,2-Dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-2-methylpropanenitrile

反応式

[CH3:1][C:2]1([CH3:13])[O:7][C:6](=[O:8])[C:5](=[C:9]([CH3:11])[CH3:10])[C:4](=[O:12])[O:3]1.[C-:14]#[N:15].[K+]>>[CH3:13][C:2]1([CH3:1])[O:3][C:4](=[O:12])[CH:5]([C:9]([CH3:10])([CH3:11])[C:14]#[N:15])[C:6](=[O:8])[O:7]1

参加物

反応物 2

HCID 9032Potassium Cyanide

HCID 752182,2-Dimethyl-5-(1-methylethylidene)-1,3-dioxane-4,6-dione

生成物 1

HCID 594965862-(2,2-Dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-2-methylpropanenitrile

実験手順

This compound was prepared by using procedures analogous to those described for the synthesis of Example 120, Step 2 starting from 2,2-dimethyl-5-(1-methylethylidene)-1,3-dioxane-4,6-dione and potassium cyanide.

後処理

customThis compound was prepared

出典と根拠

ORDレコード: ord-eb4c74cec5c44ed9a75aea60bc4485a4
出典データセット: uspto-grants-2013_07
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08481732B2

反応ノート

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