Benzaldehyde → 5-Benzylidene-2,2-dimethyl-1,3-dioxane-4,6-dione

反応式

[CH:1](=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:9][C:10]1([CH3:18])[O:15][C:14](=[O:16])[CH2:13][C:12](=[O:17])[O:11]1>>[CH:1](=[C:13]1[C:14](=[O:16])[O:15][C:10]([CH3:18])([CH3:9])[O:11][C:12]1=[O:17])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

参加物

反応物 2

HCID 240Benzaldehyde

HCID 162492,2-Dimethyl-1,3-dioxane-4,6-dione

生成物 1

HCID 5998885-Benzylidene-2,2-dimethyl-1,3-dioxane-4,6-dione

実験手順

This compound was prepared by using procedures analogous to those described for the synthesis of Example 120, Step 1 starting from benzaldehyde and 2,2-dimethyl-1,3-dioxane-4,6-dione.

後処理

customThis compound was prepared

出典と根拠

ORDレコード: ord-8a810ee49e944807acc685f32066618d
出典データセット: uspto-grants-2013_07
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08481732B2

反応ノート

読み込み中…