化工社化工社 化学情報印刷レポート · 研究参考用
Adipic Acid → 6-(2,3-Dichlorophenyl)-1,2,4-triazine-3,5-diamine;hexanedioate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Adipic Acid | HCID 196 | — |
| 反応物 | Lamotrigine | HCID 3878 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 6-(2,3-Dichlorophenyl)-1,2,4-triazine-3,5-diamine;hexanedioate | HCID 86632322 | — |
反応手順
16 mg of lamotrigine was dissolved in 2 ml of methanol, 11 mg of adipic acid was added to the solution to form a single solution. The solution was then allowed to stand for several hours to effect the slow evaporation of solvent. The solids gathered were stored in screw cap vials for subsequent analysis.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08486927B2 |
| 出典データセット | uspto-grants-2013_07 |
| ORD ID | ord-9374823017d143f1a784e1a60c0199c4 |
| 出典メモ | uspto-grants-2013_07 |