化工社化工社 化学情報印刷レポート · 研究参考用
Hydroxylamine → 1-[6-(Hydroxymethyl)pyridin-2-yl]ethanone oxime
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydroxylamine | HCID 787 | — |
| 反応物 | 1-(6-(Hydroxymethyl)pyridin-2-yl)ethanone | HCID 10329447 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 1-[6-(Hydroxymethyl)pyridin-2-yl]ethanone oxime | HCID 136346367 | — |
反応手順
To a solution of 1643 mg of 1-[6-(hydroxymethyl)pyridin-2-yl]ethanone in 25 ml of ethanol was added 0.72 ml of a 50% aqueous hydroxylamine solution, followed by stirring overnight. The reaction solution was concentrated under reduced pressure to obtain 1806 mg of 1-[6-(hydroxymethyl)pyridin-2-yl]ethanone oxime as an amorphous substance.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08486970B2 |
| 出典データセット | uspto-grants-2013_07 |
| ORD ID | ord-6ef6da3a33224778a3c3124510f154e5 |
| 出典メモ | uspto-grants-2013_07 |