化工社化工社 化学情報印刷レポート · 研究参考用
Dimethyl Sulfate → N,N,N',N',N''-Pentamethylguanidine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethyl Sulfate | HCID 6497 | — |
| 反応物 | 1,1,3,3-Tetramethylguanidine | HCID 66460 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | N,N,N',N',N''-Pentamethylguanidine | HCID 139457 | — |
反応手順
Tetramethlguanidine functionalized perfluorinated polymers were further treated with dimethyl sulfate (DMS) in DMF at 90° C. for 24 hr. Pentamethylguanidine functionalized perfluorinated polymer was obtained. Guanidine functionalized perfluorinated polymers was further treated with 1 M NaOH followed by washing with water.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08492049B2 |
| 出典データセット | uspto-grants-2013_07 |
| ORD ID | ord-8ed9385d323b4c9f82d6bcd44532a8b4 |
| 出典メモ | uspto-grants-2013_07 |