化工社化工社 化学情報印刷レポート · 研究参考用
3-(3-Fluorophenyl)propionic acid → Tert-butyl [4-[[2-[3-(3-fluorophenyl)propanoyl]hydrazino]carbonyl]-2-pyridyl]carbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-(3-Fluorophenyl)propionic acid | HCID 2737489 | — |
| 反応物 | Tert-butyl [4-(hydrazinocarbonyl)-2-pyridyl]carbamate | HCID 86640026 | — |
| 生成物 | Tert-butyl [4-[[2-[3-(3-fluorophenyl)propanoyl]hydrazino]carbonyl]-2-pyridyl]carbamate | HCID 86640025 | 60% |
反応手順
In the same manner as in Reference Example 1 and using 3-(3-fluorophenyl)propionic acid instead of benzothiazole-6-carboxylic acid and tert-butyl[4-(hydrazinocarbonyl)-2-pyridyl]carbamate instead of tert-butyl carbazate, the title compound (yield 60%) was obtained as colorless crystals.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08492378B2 |
| 出典データセット | uspto-grants-2013_07 |
| ORD ID | ord-2c88286c69ad48efb8394d62cacbe8aa |
| 出典メモ | uspto-grants-2013_07 |