反応式
[C:1]([O:7][CH3:8])(=[O:6])[CH2:2][C:3]([CH3:5])=O.[CH3:9][NH2:10]>CO>[CH3:8][O:7][C:1](=[O:6])[CH:2]=[C:3]([NH:10][CH3:9])[CH3:5]参加物
4
実験手順
To a solution of methyl acetoacetate (29.4 g, 253 mmol) in MeOH (30 mL) was added methylamine (33 wt % in EtOH; 48 mL, 385 mmol) dropwise at room temperature. The reaction was stirred for 1 hour, and then concentrated and dried to give the title compound as a white crystalline solid.
後処理
- concentrationconcentrated
- customdried
出典と根拠
- ORDレコード
- ord-83d244af03f643cea719dec0d8bec63e
- 出典データセット
- uspto-grants-2013_09
- 特許番号
- US08541587B2
関連ノート
読み込み中…