N,1-Dimethylhydrazine-1-carboxamide → 1,3-dimethyl-1-[(E)-1-[3-(quinolin-6-ylmethyl)triazolo[4,5-b]pyrazin-5-yl]ethylideneamino]urea

関与物質

反応手順

The title compound was prepared in analogy to the synthesis of example 52 from 1-(1-(quinolin-6-ylmethyl)-1H-[1,2,3]triazolo[4,5-b]pyrazin-6-yl)ethanone and N,1-dimethyl-hydrazinecarboxamide. 1H-NMR (400 MHz, DMSO-d6) δ ppm 9.73 (s, 1H), 8.89 (m, 1H), 8.36 (dd, 1H), 8.03 (s, 1H), 8.00 (d, 1H), 7.53 (dd, 1H), 7.19 (m, 1H), 6.21 (s, 2H), 3.31 (s, 3H), 2.72 (d, 3H), 2.49 (d, 3H). LCMS (method B): [MH]+=390, tR=1.99 min.

情報源と証拠