関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | 5-Bromo-2-methoxyphenylacetic acid | HCID 555306 | — |
| 生成物 | Methyl 2-(5-bromo-2-methoxyphenyl)acetate | HCID 21999895 | — |
反応手順
To 5-bromo-2-methoxyphenylacetic acid (0.900 g, 3.7 mmol) in MeOH (20 mL) was added hydrogen chloride (4N in 1,4-dioxane; 4 mL), and the reaction was stirred at 80° C. for 6 hours. The mixture was then concentrated to dryness to give the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08497381B2 |
|---|
| 出典データセット | uspto-grants-2013_07 |
|---|
| ORD ID | ord-6468b8e4aa80453a951593f3be6a0500 |
|---|
| 出典メモ | uspto-grants-2013_07 |
|---|
