化工社化工社 化学情報印刷レポート · 研究参考用
2,6-Dimethyl-4-pyranone → Tetrahydro-2,6-dimethyl-4H-pyran-4-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,6-Dimethyl-4-pyranone | HCID 13862 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Tetrahydro-2,6-dimethyl-4H-pyran-4-one | HCID 70626 | — |
反応手順
2,6-Dimethyl-4H-pyran-4-one (4 g) was dissolved in ethanol (20 mL) and 10% Pd/C (400 mg) was added. The mixture was hydrogenated under H2 (1 atm) at room temperature for 25 hrs.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07186731B2 |
| 出典データセット | uspto-grants-2007_03 |
| ORD ID | ord-88100db2213d491d806e4d1ce3aa1613 |
| 出典メモ | uspto-grants-2007_03 |