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Benzenemethanamine, 2,4-dichloro-N-methyl- → 3-(6,8-Dichloro-2-ethyl-1,2,3,4-tetrahydroisoquinolin-4-yl)benzene-1-sulfonyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzenemethanamine, 2,4-dichloro-N-methyl- | HCID 485424 | — |
| 反応物 | 3-(6,8-Dichloro-2-methyl-1,2,3,4-tetrahydroisoquinolin-4-yl)benzene-1-sulfonyl chloride | HCID 86672330 | — |
| 生成物 | 3-(6,8-Dichloro-2-ethyl-1,2,3,4-tetrahydroisoquinolin-4-yl)benzene-1-sulfonyl chloride | HCID 86672345 | — |
反応手順
Using procedures outlined in Example 1 to prepare intermediate 1.6, substituting N-(2,4-dichlorobenzyl)ethanamine for 1-(2,4-dichlorophenyl)-N-methylmethanamine, the title compound was prepared as a hydrochloride salt.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08541448B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-6b9ffe09322b413fa1a1fabdbc8d32ba |
| 出典メモ | uspto-grants-2013_09 |