関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 1-Dodecanol | HCID 8193 | — |
| 反応物 | Trioctylamine | HCID 14227 | — |
| 反応物 | Ammonium Lactate | HCID 62358 | — |
| 生成物 | Lactic Acid | HCID 612 | — |
| 生成物 | Ammonium Lactate | HCID 62358 | — |
反応手順
The procedure described in Example 1 was followed except that the reaction solution consisted of 10 g of a 70% solution of ammonium lactate, 45 g tricaprylamine, and 5 g dodecanol. The reaction mixture was heated for 2 hours at 160° C. and atmospheric pressure, resulting in a conversion of about 98% from ammonium lactate to lactic acid. Some of the dodecanol also reacted with lactic acid to form an ester. The conversion from ammonium lactate to lactic acid plus lactic acid ester was about 99%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07186856B2 |
|---|
| 出典データセット | uspto-grants-2007_03 |
|---|
| ORD ID | ord-b407da3550d84f0ebf03fcad71319dc5 |
|---|
| 出典メモ | uspto-grants-2007_03 |
|---|
