化工社化工社 化学情報印刷レポート · 研究参考用
Cyclohexanepropanoic acid → HCID 178526602、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclohexanepropanoic acid | HCID 69702 | — |
| 反応物 | 2-Bromo-1-(3-nitrophenyl)ethan-1-one | HCID 75213 | — |
| 反応物 | N-(tert-butoxycarbonyl)glycine | HCID 78288 | — |
| 反応物 | 4-Azidophenacyl bromide | HCID 92627 | — |
| 生成物 | HCID 178526602 | HCID 178526602 | 26% |
反応手順
This compound is prepared according to an operating method analogous to that described for Stage 4.1 of Example 4, with cyclohexylethylcarboxylic acid and 3-nitrophenacyl bromide placing N-(tert-butoxycarbonyl)-glycine and 4-azidophenacyl bromide respectively. The expected compound is obtained in the form of a yellow powder with a yield of 26%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07192975B2 |
| 出典データセット | uspto-grants-2007_03 |
| ORD ID | ord-888ec7bdd9894376a72ebe9c688b6941 |
| 出典メモ | uspto-grants-2007_03 |