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4-Benzylphenol → (2S)-3-{4-[3-(4-Benzyl-phenoxy)-prop-1-ynyl]-phenyl}-2-methoxy-propionic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Benzylphenol | HCID 7563 | — |
| 反応物 | (2S)-3-[4-(3-Chloro-prop-1-ynyl)-phenyl]-2-methoxy-propionic acid ethyl ester | HCID 58822943 | — |
| 生成物 | (2S)-3-{4-[3-(4-Benzyl-phenoxy)-prop-1-ynyl]-phenyl}-2-methoxy-propionic acid | HCID 58822715 | — |
反応手順
The title compound was prepared from (2S)-3-[4-(3-Chloro-prop-1-ynyl)-phenyl]-2-methoxy-propionic acid ethyl ester from Example 5, Step A and 4-hydroxydiphenylmethane in a manner analogous to that described for Example 5, Step B. MS(ES) for C26H24O4[M−H]−: 399.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07192982B2 |
| 出典データセット | uspto-grants-2007_03 |
| ORD ID | ord-c258d48a801b4a52a3ab4e32ff6fc4f8 |
| 出典メモ | uspto-grants-2007_03 |