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3-Hydroxy-N-phenylaniline → (2s)-2-Methoxy-3-{4-[5-(3-phenylamino-phenoxy)-pent-1-ynyl]-phenyl}-propionic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Hydroxy-N-phenylaniline | HCID 7546 | — |
| 反応物 | 3-[4-(5-Bromo-pent-1-ynyl)-phenyl]-2-methoxy-propionic acid ethyl ester | HCID 69421973 | — |
| 生成物 | (2s)-2-Methoxy-3-{4-[5-(3-phenylamino-phenoxy)-pent-1-ynyl]-phenyl}-propionic acid | HCID 59015146 | — |
反応手順
The title compound was prepared from 3-[4-(5-Bromo-pent-1-ynyl)-phenyl]-2-methoxy-propionic acid ethyl ester from Example 24 Step A and 3-hydroxydiphenylamine in a manner analogous to that described for Example 24, Step B. MS(ES) for C27H27NO4[M+H]+:430.2.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07192982B2 |
| 出典データセット | uspto-grants-2007_03 |
| ORD ID | ord-92b2bc762cc142678fab7bee0b5c8e35 |
| 出典メモ | uspto-grants-2007_03 |