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Aniline → 3-(4-methoxyphenyl)-4-phenyl-5-methyl-4H-1,2,4-triazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | N'-acetyl-4-methoxybenzohydrazide | HCID 839858 | — |
| 反応物 | Phosphorus | HCID 5462309 | — |
| 溶媒 | 1,2-Dichlorobenzene | HCID 7239 | — |
| 生成物 | 3-(4-methoxyphenyl)-4-phenyl-5-methyl-4H-1,2,4-triazole | HCID 13054023 | — |
反応手順
Using the procedure of Step B in Example 1, 26.3 ml of aniline, 150 ml of o-dichlorobenzene, 4.65 ml of phosphorus trichlorode and 10 g of N-(4-methoxybenzoyl)-N'-acetyl-hydrazine [prepared by process of J. Org., Vol. 19 (1954), p. 194-201] were reacted to obtain 7.1 g of 3-(4-methoxyphenyl)-4-phenyl-5-methyl -4H-1,2,4-triazole melting at 140°-141° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04727084 |
| 出典データセット | uspto-grants-1988_02 |
| ORD ID | ord-afd7c470aaa9450c98ccacd72a59e875 |
| 出典メモ | uspto-grants-1988_02 |