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Benzyl Bromide → 3-(Benzyloxy)-2-bromo-6-iodopyridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzyl Bromide | HCID 7498 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 2-Bromo-6-iodopyridin-3-ol | HCID 10979479 | — |
| 生成物 | 3-(Benzyloxy)-2-bromo-6-iodopyridine | HCID 11025563 | — |
反応手順
2-Bromo-6-iodopyridin-3-ol was reacted with potassium carbonate and benzyl bromide to obtain 3-(benzyloxy)-2-bromo-6-iodopyridine, which was then reacted in a similar manner to Reference Example 11, Example 22 and Example 4, successively. Further, the resulting product was subjected to catalytic reduction using palladium/carbon to obtain an objective compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07196080B2 |
| 出典データセット | uspto-grants-2007_03 |
| ORD ID | ord-16b798cbc5e24f36bb7af0c1f45380de |
| 出典メモ | uspto-grants-2007_03 |