化工社化工社 化学情報印刷レポート · 研究参考用
Borohydride → 4-Methoxy-3-(4-methoxyphenyl)benzyl alcohol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Borohydride | HCID 28123 | — |
| 反応物 | 6,4'-Dimethoxybiphenyl-3-carbaldehyde | HCID 22391191 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 4-Methoxy-3-(4-methoxyphenyl)benzyl alcohol | HCID 68841639 | 87.2% |
反応手順
A solution of 4-methoxy-3-(4-methoxyphenyl)benzenecarboxaldehyde (1 g, 4.13 mmol) in methanol (12 mL) was treated with polymer-supported borohydride (10.3 mmol) and the mixture shaken for 16 hours. The resin was then filtered and the filtrate concentrated under reduced pressure to afford 0.88 g of title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07196102B2 |
| 出典データセット | uspto-grants-2007_03 |
| ORD ID | ord-a9f128eb66ba4a03a994df7c3c66eb4c |
| 出典メモ | uspto-grants-2007_03 |