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5-Methoxyindan-1-one → 2-(6-methoxy-1H-inden-3-yl)propanoic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Methoxyindan-1-one | HCID 78787 | — |
| 反応物 | Methyl 2-bromopropionate | HCID 95576 | — |
| 生成物 | 2-(6-methoxy-1H-inden-3-yl)propanoic Acid | HCID 21942769 | 68% |
反応手順
This substrate was prepared using the same procedures as described for Examples 1 and 2a, starting with 5-methoxyl-1-indanone and methyl 2-bromopropionate. Yield: 68%. 1H NMR (CD2Cl2) δ 7.34 (d, J=9, 1H), 7.07 (d, J=2, 1H), 6.85 (dd, J=9, J=2, 1H), 6.32 (m, 1H), 3.82 (m, 4H), 3.36 (m, 2H), 1.56 (d, J=7, 3H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08541618B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-798cad91915e4029b13d37a40ba46f77 |
| 出典メモ | uspto-grants-2013_09 |