化工社化工社 化学情報印刷レポート · 研究参考用
Sulfuric Acid → Benzene, ethenyl-, polymer with 1,3-butadiene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | Styrene | HCID 7501 | — |
| 反応物 | 1,3-Butadiene | HCID 7845 | — |
| 反応物 | Tetrasodium Pyrophosphate | HCID 24403 | — |
| 反応物 | (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 107526 | — |
| 反応物 | Potassium Oleate | HCID 23665571 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Benzene, ethenyl-, polymer with 1,3-butadiene | HCID 62697 | — |
反応手順
50 parts of butadiene rubber latex powder, 50 parts of styrene and 150 parts of deionized water were blended. To the blend, 1.0 parts of potassium oleate, 0.4 parts of cumenhydroperoxide, 0.2 parts of mercaptan-containing chain transfer agent, 0.4 parts of glucose, 0.01 parts of ferrous sulfate hydrate, and 0.3 parts of sodium pyrophosphate were added. The blend was kept at 75° C. for 5 hours to obtain g-ABS latex. To the g-ABS latex, 0.4 parts of sulfuric acid was added, coagulated and dried to obtain butadiene-styrene graft copolymer resin (g-BS) in a powder form.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07196126B2 |
| 出典データセット | uspto-grants-2007_03 |
| ORD ID | ord-6c240420062249dfb41ba0ba3e9b74eb |
| 出典メモ | uspto-grants-2007_03 |