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4-(Naphthalen-2-yl)piperidine → ethyl (S)-7-(2-hydroxy-3-(4-(naphthalen-2-yl)piperidino)propyloxy)benzo(b)furan-2-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(Naphthalen-2-yl)piperidine | HCID 22029264 | — |
| 反応物 | ethyl (S)-7-(glycidyloxy)benzo(b)furan-2-carboxylate | HCID 86585640 | — |
| 生成物 | ethyl (S)-7-(2-hydroxy-3-(4-(naphthalen-2-yl)piperidino)propyloxy)benzo(b)furan-2-carboxylate | HCID 60077908 | 77.3% |
反応手順
By the reactions in the same manner as in Starting Material Synthesis Example 11 using ethyl (S)-7-(glycidyloxy)benzo(b)furan-2-carboxylate (5.3 g) and 4-(naphthalen-2-yl)piperidine (3.0 g), the title compound (5.2 g) was obtained as a brown oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07196199B2 |
| 出典データセット | uspto-grants-2007_03 |
| ORD ID | ord-21b098ff6bb2424684f71519495d1967 |
| 出典メモ | uspto-grants-2007_03 |