Thiourea, N,N'-di-2-propen-1-yl- → 3-Allyl-2-allylimino-(3,4-dimethyl-5-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrobromide
反応式
[Br:1][CH2:2][C:3]([C:5]1[CH:10]=[C:9]([S:11](=[O:14])(=[O:13])[NH2:12])[C:8]([CH3:15])=[C:7]([CH3:16])[CH:6]=1)=[O:4].[CH2:17]([NH:20][C:21]([NH:23][CH2:24][CH:25]=[CH2:26])=[S:22])[CH:18]=[CH2:19]>>[BrH:1].[CH2:24]([N:23]1[C:3]([C:5]2[CH:10]=[C:9]([S:11](=[O:14])(=[O:13])[NH2:12])[C:8]([CH3:15])=[C:7]([CH3:16])[CH:6]=2)([OH:4])[CH2:2][S:22][C:21]1=[N:20][CH2:17][CH:18]=[CH2:19])[CH:25]=[CH2:26]参加物
3
実験手順
was obtained in a manner analogous to the method described in Example 6 in amorphous form from 3.1 g of 2-bromo-3',4'-dimethyl-5'-sulfamoyl-acetophenone and 1.6 g of 1,3-diallyl-thiourea and the substance was brought to crystallization under ether. M.p. 138°-140° C (decomposition).
後処理
- customwas obtained in a manner analogous to the method
- customthe substance was brought to crystallization under ether