3-Pentyn-2-ol, 1-(4-fluorophenoxy)-5-[(tetrahydro-2H-pyran-2-yl)oxy]-, 2-acetate → HCID 22759281、化合物

HRID 460844ノート

反応式

HRID 460844 の反応式
O1CCCCC1[O:7][CH2:8][C:9]#[C:10][CH:11]([O:21][C:22](=[O:24])[CH3:23])[CH2:12][O:13][C:14]1[CH:19]=[CH:18][C:17]([F:20])=[CH:16][CH:15]=1.O1CCCCC1OCCCC(OC(=O)C)COC1C=CC(F)=CC=1>>[C:22]([O:21][CH:11]([CH2:12][O:13][C:14]1[CH:19]=[CH:18][C:17]([F:20])=[CH:16][CH:15]=1)[C:10]#[C:9][CH2:8][OH:7])(=[O:24])[CH3:23]

参加物

3

反応物 2

HCID 227592583-Pentyn-2-ol, 1-(4-fluorophenoxy)-5-[(tetrahydro-2H-pyran-2-yl)oxy]-, 2-acetateHCID 22759299HCID 22759299、化合物

生成物 1

HCID 22759281HCID 22759281、化合物

実験手順

This compound is prepared by the procedure described in Example 4, Step B-5, except that 1-(2-tetrahydropyranyloxy)-4-acetoxy-5-(4-fluorophenoxy)-2-pentyne (Example 4, Step B-3) is substituted for 1-(2-tetrahydropyranyloxy)-4-acetoxy-5-(4-fluorophenoxy)pentane. The title compound is obtained as a light yellow oil which is not distilled but used directly in the next step.

後処理

  1. customThis compound is prepared by the procedure

出典と根拠

ORDレコード
ord-b4bd90c43d3849008576d055b7ecd810
出典データセット
uspto-grants-1977_12
特許番号
US04061643

反応ノート

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