Phenol → 8-Acetyl-12-hydroxy-13-phenoxytridecanoic acid

反応式

C1(O)C=CC=CC=1.[C:8]([CH:11]([CH2:21][CH2:22][CH2:23][CH:24]([OH:37])[CH2:25][O:26][C:27]1[CH:32]=[CH:31][C:30](C(C)(C)C)=[CH:29][CH:28]=1)[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][C:18]([OH:20])=[O:19])(=[O:10])[CH3:9]>>[C:8]([CH:11]([CH2:21][CH2:22][CH2:23][CH:24]([OH:37])[CH2:25][O:26][C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1)[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][C:18]([OH:20])=[O:19])(=[O:10])[CH3:9]

参加物

反応物 2

HCID 996Phenol

HCID 22759343HCID 22759343、化合物

生成物 1

HCID 227592678-Acetyl-12-hydroxy-13-phenoxytridecanoic acid

実験手順

The synthesis of this compound is carried out by the procedure of Example 10 except that an equivalent amount of phenol is substituted for the 4-tert-butylphenol of Example 10. The title compound is obtained as a colorless viscous oil after purification by silica gel column chromatography.

後処理

customThe synthesis of this compound

出典と根拠

ORDレコード: ord-ea859b1c4cb24ab8ae748021be14a843
出典データセット: uspto-grants-1977_12
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04061643

反応ノート

読み込み中…