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Cyclohexylamine, 2-phenyl-, hydrochloride, trans- → N-[(1R,2S)-2-phenylcyclohexyl]azepan-2-imine;hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclohexylamine, 2-phenyl-, hydrochloride, trans- | HCID 209556 | — |
| 反応物 | rac-(1R,2R)-2-phenylcyclopentan-1-amine hydrochloride | HCID 70051154 | — |
| 生成物 | N-[(1R,2S)-2-phenylcyclohexyl]azepan-2-imine;hydrochloride | HCID 145795666 | — |
反応手順
Following the procedure of Example 23, only substituting for cis-2-phenylcyclopentylamine hydrochloride an appropriate amount of trans-2-phenylcyclohexylamine hydrochloride, M.P. 251° -257° C, and employing a reaction time of 38 days, the desired product is obtained, M.P. 236°-239° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04061746 |
| 出典データセット | uspto-grants-1977_12 |
| ORD ID | ord-7df08f1c2d934730b4e4341281fc2bf8 |
| 出典メモ | uspto-grants-1977_12 |