反応式
[ClH:1].[C:2]1([C@H:8]2[CH2:12][CH2:11][CH2:10][C@H:9]2[NH2:13])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.COC1[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][N:22]=1.Cl.C1([C@H]2CCC[C@H]2N)CCCCC1.COC1CCCCN=1>>[ClH:1].[CH:2]1([C@H:8]2[CH2:12][CH2:11][CH2:10][C@H:9]2[N:13]=[C:21]2[CH2:20][CH2:19][CH2:18][CH2:17][NH:22]2)[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1参加物
5
実験手順
Following the procedure of Example 23, only substituting for cis-2-phenylcyclopentylamine hydrochloride and O-methylcaprolactim, appropriate amounts of cis-2-(cyclohexyl)cyclopentylamine hydrochloride and O-methylvalerolactim respectively the desired product is obtained, M.P. 195.5°-197° C.
出典と根拠
- ORDレコード
- ord-f7e359947188445885dbe2d74e1dd436
- 出典データセット
- uspto-grants-1977_12
- 特許番号
- US04061746
関連ノート
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