化工社化工社 化学情報印刷レポート · 研究参考用
N,N'-Dibutylthiourea → 3-n-Butyl-2-n-butylimino-4-(4-chloro-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrobromide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N,N'-Dibutylthiourea | HCID 2723622 | — |
| 反応物 | Bromo-4'-chloro-3'-sulfamoylacetophenone | HCID 12952390 | — |
| 生成物 | 3-n-Butyl-2-n-butylimino-4-(4-chloro-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrobromide | HCID 22760686 | — |
反応手順
6.2 g of 2 bromo-4'-chloro-3'-sulfamoylacetophenone were reacted with 3.8 g of 1,3-di-n-butylthiourea according to the prescription given in Example 12 and the end product was precipitated with diisopropyl ether.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04061761 |
| 出典データセット | uspto-grants-1977_12 |
| ORD ID | ord-d513453921a64e1bac66ba1a16b15356 |
| 出典メモ | uspto-grants-1977_12 |