N,N'-Dibutylthiourea → 3-n-Butyl-2-n-butylimino-4-(4-chloro-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride

HRID 461118ノート

反応式

HRID 461118 の反応式
[Cl:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH2:16]([NH:20][C:21]([NH:23][CH2:24][CH2:25][CH2:26][CH3:27])=[S:22])[CH2:17][CH2:18][CH3:19]>>[ClH:1].[CH2:24]([N:23]1[C:3]([C:5]2[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=2)([OH:4])[CH2:2][S:22][C:21]1=[N:20][CH2:16][CH2:17][CH2:18][CH3:19])[CH2:25][CH2:26][CH3:27]

参加物

3

反応物 2

HCID 2723622N,N'-DibutylthioureaHCID 21316749HCID 21316749、化合物

生成物 1

HCID 227606883-n-Butyl-2-n-butylimino-4-(4-chloro-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride

実験手順

5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone were reacted with 3.8 g of 1,3-di-n-butylthiourea according to the prescription given in Example 12 and the end product was precipitated with diisopropyl ether.

後処理

  1. customthe end product was precipitated with diisopropyl ether

出典と根拠

ORDレコード
ord-58ff00f1d9ae47068b247a3bdca91b65
出典データセット
uspto-grants-1977_12
特許番号
US04061761

反応ノート

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