1-Cyclohexyl-3-methylthiourea → HCID 22760421、化合物
反応式
[Br:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH:16]1([NH:22][C:23]([NH:25][CH3:26])=[S:24])[CH2:21][CH2:20][CH2:19][CH2:18][CH2:17]1>>[BrH:1].[Cl:11][C:8]1[CH:9]=[CH:10][C:5]([C:3]2([OH:4])[CH2:2][S:24][C:23](=[N:22][CH:16]3[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21]3)[N:25]2[CH3:26])=[CH:6][C:7]=1[S:12](=[O:15])(=[O:14])[NH2:13]参加物
3
実験手順
4.7 g of 2-bromo-4'-chloro-3'-sulfamoylacetophenone were reacted with 2.6 g of 1-cyclohexyl-3-methylthiourea in the manner described in Example 23 and the colorless crystalline end product was filtered off. Melting point: 178° C (decomposition).
後処理
- filtrationthe colorless crystalline end product was filtered off
出典と根拠
- ORDレコード
- ord-5b70492fb96b4c6c996544be08192c71
- 出典データセット
- uspto-grants-1977_12