Diisopropylthiourea → HCID 22760621、化合物

HRID 461158

反応式

HRID 461158 の反応式
[Cl:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH:16]([NH:19][C:20]([NH:22][CH:23]([CH3:25])[CH3:24])=[S:21])([CH3:18])[CH3:17]>>[ClH:1].[CH:23]([N:22]1[C:3]([C:5]2[CH:10]=[CH:9][C:8]([CH3:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=2)([OH:4])[CH2:2][S:21][C:20]1=[N:19][CH:16]([CH3:18])[CH3:17])([CH3:25])[CH3:24]

参加物

3

反応物 2

HCID 2758386DiisopropylthioureaHCID 136287832-Chloro-4'-methyl-3'-sulfamoylacetophenone

生成物 1

HCID 22760621HCID 22760621、化合物

実験手順

5 g of 2-chloro-4'-methyl-3'-sulfamoylacetophenone and 3.2 g of 1,3-diisopropyl thiourea were reacted as prescribed in Example 12 and worked up according to Example 67d). Colorless crystals, melting point: 152° C (decomposition).

出典と根拠

ORDレコード
ord-7bac6b1dea9148f58fe92baf9ec13592
出典データセット
uspto-grants-1977_12
特許番号
US04061761

関連ノート

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