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Thionyl Chloride → 3-Sulfamoylbenzoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 3-Sulfamoylbenzoic acid | HCID 229352 | — |
| 生成物 | 3-Sulfamoylbenzoyl chloride | HCID 18801883 | — |
反応手順
10 g of ground 3-sulfamoylbenzoic acid were reacted as prescribed in Example 70b), the thionyl chloride was distilled off and the residue was crystallized under a mixture of petroleum ether and diethyl ether (1:1). Melting point: 123° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04061761 |
| 出典データセット | uspto-grants-1977_12 |
| ORD ID | ord-fd25773f3f24442092591b5bfa79d79e |
| 出典メモ | uspto-grants-1977_12 |