化工社化工社 化学情報印刷レポート · 研究参考用
Water → HCID 24708775、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Allyl bromide | HCID 7841 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 4-(4'-Hydroxyphenyl)-2-butanone | HCID 21648 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | HCID 24708775 | HCID 24708775 | — |
反応手順
p-Hydroxy benzylacetone (1.5 g.), KOH (6 g.) and allyl bromide (1.2 g.) were stirred in ethanol (50 ml) overnight. Water was added and the mixture extracted with ether, which was evaporated to give the compound (1.6 g.) as an oil purified by column chromatography.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04062978 |
| 出典データセット | uspto-grants-1977_12 |
| ORD ID | ord-67502816a83c4a06a3fe4d307df71c29 |
| 出典メモ | uspto-grants-1977_12 |