化工社化工社 化学情報印刷レポート · 研究参考用
Allyl iodide → Allyl Hexadecyl Dimethyl Ammonium Iodide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Allyl iodide | HCID 11166 | — |
| 反応物 | Dimethylhexadecylamine | HCID 16221 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | Allyl Hexadecyl Dimethyl Ammonium Iodide | HCID 21391586 | — |
反応手順
16.8 grams of allyl iodide were dissolved in 44.6 grams of ethyl acetate and 27.8 grams of dimethyl hexadecyl amine were added slowly with stirring at room temperature. Within 15 minutes after the addition of the amine was complete, the viscosity of the solution increased and crystallization occurred. After 24 hours the crystals were filtered, washed with ethyl acetate, and dried. The colorless crystalline product contained 88% of the theoretical amount of iodide ion.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04064091 |
| 出典データセット | uspto-grants-1977_12 |
| ORD ID | ord-8acba59821c743c79df5910d30972d67 |
| 出典メモ | uspto-grants-1977_12 |