化工社化工社 化学情報印刷レポート · 研究参考用
Cyclohexyl bromide → Cyclohexyldicyclohexylphosphinodithioate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclohexyl bromide | HCID 7960 | — |
| 反応物 | Phosphinodithioic acid, dicyclohexyl- | HCID 75641 | — |
| 生成物 | Cyclohexyldicyclohexylphosphinodithioate | HCID 21391611 | — |
反応手順
Cyclohexylbromide was reacted with the ammonium salt of dicyclohexylphosphinodithioic acid to obtain cyclohexyldicyclohexylphosphinodithioate, m.p. 82°-85° C, which on testing lasted 1250 hours* longer than the control. The average number of hours required to reach failure was 3.5 times that of the control.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04064106 |
| 出典データセット | uspto-grants-1977_12 |
| ORD ID | ord-b4436844ded644a6b23e9bb82fa7c71b |
| 出典メモ | uspto-grants-1977_12 |