Butyl bromide → n-Butyl dicyclohexylphosphinodithioate

HRID 461611

反応式

HRID 461611 の反応式
[CH2:1](Br)[CH2:2][CH2:3][CH3:4].[CH:6]1([P:12]([CH:15]2[CH2:20][CH2:19][CH2:18][CH2:17][CH2:16]2)([SH:14])=[S:13])[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1>>[CH:6]1([P:12]([CH:15]2[CH2:20][CH2:19][CH2:18][CH2:17][CH2:16]2)([S:14][CH2:1][CH2:2][CH2:3][CH3:4])=[S:13])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11]1

参加物

3

実験手順

n-Butyl bromide was reacted with the ammonium salt of dicyclohexylphosphinodithioic acid to obtain n-butyl dicyclohexylphosphinodithioate, a viscous liquid, b.p. 167°-175° C at 0.15 mm., which on testing lasted 900 hours longer than the control. The total number of hours required to reach failure was 2.8 times that of the control.

出典と根拠

ORDレコード
ord-e1db73a18904424688880971386e357f
出典データセット
uspto-grants-1977_12
特許番号
US04064106

関連ノート

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