Phosphinodithioic acid, dicyclohexyl- → Isotridecyl dicyclohexylphosphinodithioate

HRID 461612

反応式

HRID 461612 の反応式
[CH3:1][CH:2]([CH3:14])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12]Br.[CH:15]1([P:21]([CH:24]2[CH2:29][CH2:28][CH2:27][CH2:26][CH2:25]2)([SH:23])=[S:22])[CH2:20][CH2:19][CH2:18][CH2:17][CH2:16]1>>[CH:15]1([P:21]([CH:24]2[CH2:29][CH2:28][CH2:27][CH2:26][CH2:25]2)([S:23][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH:2]([CH3:14])[CH3:1])=[S:22])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20]1

参加物

3

反応物 2

HCID 75641Phosphinodithioic acid, dicyclohexyl-HCID 155697271-Bromo-11-methyldodecane

生成物 1

HCID 54099874Isotridecyl dicyclohexylphosphinodithioate

実験手順

11-Methyldodecyl bromide was reacted with the ammonium salt of dicyclohexylphosphinodithioic acid to obtain isotridecyl dicyclohexylphosphinodithioate, a viscous colorless liquid, which on testing lasted 750 hours longer than the control. The total number of hours required to reach failure was 2.6 times that of the control.

出典と根拠

ORDレコード
ord-9bf3647e143b4278858c27746ec81b5e
出典データセット
uspto-grants-1977_12
特許番号
US04064106

関連ノート

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