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2,4-Dichloro-6-nitroaniline → 10,12-Dichlorodibenzo[a,c]phenazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,4-Dichloro-6-nitroaniline | HCID 75893 | — |
| 反応物 | 1,2-Phenanthrenedione | HCID 3080566 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | 10,12-Dichlorodibenzo[a,c]phenazine | HCID 21391728 | 81% |
反応手順
When 0.12 mole each of 2,4-dichloro-6-nitroaniline and phenanthrenequinone were reacted by the method of Example 1, 24 g. (81 percent yield) of 10,12-dichlorodibenzo[a,c]phenazine, mp = 221°-222° C. (acetone), were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04064127 |
| 出典データセット | uspto-grants-1977_12 |
| ORD ID | ord-cf5c608cf4994a89b522be502c1d94b8 |
| 出典メモ | uspto-grants-1977_12 |