Methanol → HCID 178512939、化合物
反応式
[NH2:1][C@H:2]([C:10]([OH:12])=[O:11])[CH2:3][CH2:4][CH2:5][NH:6][C:7](=[NH:9])[NH2:8].[OH:13][P:14]([F:17])([OH:16])=[O:15].O.CO>C(O)C>[P:14]([F:17])([OH:16])([OH:15])=[O:13].[NH2:1][C@H:2]([C:10]([OH:12])=[O:11])[CH2:3][CH2:4][CH2:5][NH:6][C:7](=[NH:8])[NH2:9]参加物
6
実験手順
L-arginine monofluorophosphate was prepared by combining 34.8 gm. of free-base L-arginine with 20 gm. of monofluorophosphoric acid in about 75 ml. of water. The resulting clear syrup was poured into 750 ml. of a mixture of methanol and ethanol. This was allowed to stand over night and the salt was collected by filtration. The resulting L-arginine monofluorophosphate was then rinsed with methanol and air dried.
後処理
- additionThe resulting clear syrup was poured into 750 ml
- waitto stand over night
- filtrationthe salt was collected by filtration
- washThe resulting L-arginine monofluorophosphate was then rinsed with methanol and air
- customdried
出典と根拠
- ORDレコード
- ord-04641c77270a470094c99656595ec83f
- 出典データセット
- uspto-grants-1977_12
- 特許番号
- US04064138
反応ノート
読み込み中…