Water → HCID 178511811、化合物
反応式
[NH2:1][C@H:2]([C:9]([OH:11])=[O:10])[CH2:3][C:4]1[N:8]=[CH:7][NH:6][CH:5]=1.[OH:12][P:13]([F:16])([OH:15])=[O:14].O>CO.C(O)C>[P:13]([F:16])([OH:15])([OH:14])=[O:12].[NH2:1][C@H:2]([C:9]([OH:11])=[O:10])[CH2:3][C:4]1[N:8]=[CH:7][NH:6][CH:5]=1参加物
5
実験手順
L-histidine monofluorophosphate was prepared by combining 31 gm. of free-base L-histidine with 20 gm. of monofluorophosphoric acid in about 75 ml. of water. A clear syrup resulted. The syrup was poured into 750 ml. of a methanol-ethanol mixture. The precipitate (L-histidine monofluorophosphate) was collected and vacuum dried in a desiccator.
後処理
- customA clear syrup resulted
- additionThe syrup was poured into 750 ml
- customThe precipitate (L-histidine monofluorophosphate) was collected
- customvacuum dried in a desiccator
出典と根拠
- ORDレコード
- ord-17e90312b2714341854be25add764976
- 出典データセット
- uspto-grants-1977_12
- 特許番号
- US04064138
反応ノート
読み込み中…