化工社化工社 化学情報印刷レポート · 研究参考用
Methylhydrazine → 5-Bromo-2-propyl-1,3-diethylisoindole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methylhydrazine | HCID 6061 | — |
| 反応物 | Hydrazine, propyl- | HCID 42007 | — |
| 反応物 | 1,2-Dipropylbenzene | HCID 186151 | — |
| 反応物 | Cyclopropylhydrazine | HCID 19594968 | — |
| 反応物 | 4-Bromo-1,2-dipropylbenzene | HCID 21392121 | — |
| 生成物 | 5-Bromo-2-propyl-1,3-diethylisoindole | HCID 21392144 | — |
反応手順
Following the procedure of Example 3, Step A, except that the o-dipropylbenzene of Example 3 is replaced by an equivalent amount of: 4-chloro-; 4-iodo-; and 4-bromo-1,2-dipropylbenzene and the methylhydrazine is replaced by an equivalent amount of propylhydrazine; cyclopropylhydrazine; and γ-THP-oxy-propylhydrazine, there is obtained 5-chloro, 5-iodo, and 5-bromo-2-propyl-1,3-diethylisoindole; 5-chloro-; 5-iodo-; and 5-bromo-2-cyclopropyl-1,3-diethylisoindole; and 5-chloro-; 5-iodo-; and 5-bromo-2-γ-THP-oxy-propyl-1,3-diethylisoindole, respectively; wherein THP represents tetrahydropyranyloxy.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04064139 |
| 出典データセット | uspto-grants-1977_12 |
| ORD ID | ord-877e129cfda0459e98ea2a4495e18143 |
| 出典メモ | uspto-grants-1977_12 |