化工社化工社 化学情報印刷レポート · 研究参考用
Bromine → 3-Bromo-5-tert-butyl-4-hydroxybenzaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Bromine | HCID 24408 | — |
| 反応物 | 3-(tert-Butyl)-4-hydroxybenzaldehyde | HCID 3017618 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | 3-Bromo-5-tert-butyl-4-hydroxybenzaldehyde | HCID 14839297 | — |
反応手順
To 3-tert-butyl-4-hydroxybenzaldehyde (3 gm) in acetic acid (30 ml) was added dropwise bromine (1.5 ml). The mixture was stirred at 25° for 3 hours and the solvent removed in vacuo. Recrystallisation of the residue from aqueous ethanol gave 3-bromo-5-tert-butyl-4-hydroxybenzaldehyde (3.2 gm) m.p. 126°.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04064266 |
| 出典データセット | uspto-grants-1977_12 |
| ORD ID | ord-4e6b889b26734e6b98e2c03dea89c9c8 |
| 出典メモ | uspto-grants-1977_12 |