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Ethyl 3-furoate → N-{2-[2-(1-Methylpiperidin-2-yl)ethyl]phenyl}furan-3-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl 3-furoate | HCID 69201 | — |
| 反応物 | 2-(2-Aminophenethyl)-1-methylpiperidine | HCID 11085282 | — |
| 生成物 | N-{2-[2-(1-Methylpiperidin-2-yl)ethyl]phenyl}furan-3-carboxamide | HCID 20559948 | — |
反応手順
Reaction of ethyl furan-3-carboxylate prepared by the method of Boyd et al, Synthesis, 545, (Oct. 1971) with 2-(2-aminophenethyl)-1-methylpiperidine according to the procedure of Example 115 provides 2'-[2-(1-methyl-2-piperidyl)ethyl]-3-furancarboxanilide, m.p. 114.5°-115.5° C (corr.), from isopropyl ether and then ethyl acetate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04064254 |
| 出典データセット | uspto-grants-1977_12 |
| ORD ID | ord-eb113b11603b47ca95fa7093ff3a8dc0 |
| 出典メモ | uspto-grants-1977_12 |