化工社化工社 化学情報印刷レポート · 研究参考用
Isopropylamine → 2-chloroethanephosphonic acid isopropyl ester N-monoisopropylamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isopropylamine | HCID 6363 | — |
| 反応物 | (2-Chloroethyl)phosphonic dichloride | HCID 69645 | — |
| 反応物 | 2-chloroethanephosphonic acid N-monoisopropylamide chloride | HCID 86735308 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 2-chloroethanephosphonic acid isopropyl ester N-monoisopropylamide | HCID 86735309 | — |
反応手順
The 2-chloroethane-phosphonic acid N-mono-isopropylamide chloride used as starting product was prepared from 2-chloroethane-phosphonic acid dichloride and iso-propylamine in toluene at 0° C. Yield: 91% of the theory, nD28 = 1.4854.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04065288 |
| 出典データセット | uspto-grants-1977_12 |
| ORD ID | ord-6d8821fac516425287dcfb50e1433db5 |
| 出典メモ | uspto-grants-1977_12 |