化工社化工社 化学情報印刷レポート · 研究参考用
N-(3-(dimethylamino)propyl)formamide → N,N-dimethyl-N-(4-nitrophenyl)carbamylmethyl-N-3-formamidopropylammonium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-(3-(dimethylamino)propyl)formamide | HCID 80020 | — |
| 反応物 | Acetanilide, 2-chloro-4'-nitro- | HCID 140220 | — |
| 溶媒 | Isopropanol | HCID 3776 | — |
| 生成物 | N,N-dimethyl-N-(4-nitrophenyl)carbamylmethyl-N-3-formamidopropylammonium chloride | HCID 86733006 | — |
反応手順
In a manner similar to that described above in 1a, and using 14.2 parts of N-(3-dimethylaminopropyl)formamide, 20.0 parts of 2-chloro-4'-nitroacetanilide, and 78 parts of isopropyl alcohol there was obtained 27.4 parts of N,N-dimethyl-N-(4-nitrophenyl)carbamylmethyl-N-3-formamidopropylammonium chloride as a white solid which melted at 195°-196° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04065500 |
| 出典データセット | uspto-grants-1977_12 |
| ORD ID | ord-402c1ace94fc4ca599dadaf99a086bcf |
| 出典メモ | uspto-grants-1977_12 |