化工社化工社 化学情報印刷レポート · 研究参考用
Tert-Butylamine → 2-(2-t-Butylamino-5-thiadiazolyl)-1-methyl-5-nitroimidazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Tert-Butylamine | HCID 6385 | — |
| 反応物 | Cyclohexylamine | HCID 7965 | — |
| 反応物 | 2-(2-Cyclohexylamino-5-thiadiazolyl)-1-methyl-5nitroimidazole | HCID 21390861 | — |
| 生成物 | 2-(2-t-Butylamino-5-thiadiazolyl)-1-methyl-5-nitroimidazole | HCID 21390806 | — |
反応手順
The preparation of the above compound is accomplished essentially by the procedure described for the 2-cyclohexylamino derivative (Example 38), an equivalent of t-butylamine replacing the cyclohexylamine. Recrystallization of the crude product from a mixture of ethyl acetate and acetone gives the pure compound melting at 249°-251° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04065567 |
| 出典データセット | uspto-grants-1977_12 |
| ORD ID | ord-73ab2a9a9569489d90ea3ede1479815f |
| 出典メモ | uspto-grants-1977_12 |