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Cyclohexylamine → 2-(2-n-Octylamino-5-thiadiazolyl)-1-methyl-5-nitroimidazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclohexylamine | HCID 7965 | — |
| 反応物 | Octylamine | HCID 8143 | — |
| 反応物 | 2-(2-Cyclohexylamino-5-thiadiazolyl)-1-methyl-5nitroimidazole | HCID 21390861 | — |
| 生成物 | 2-(2-n-Octylamino-5-thiadiazolyl)-1-methyl-5-nitroimidazole | HCID 68120260 | — |
反応手順
The preparation of the above compound is carried out essentially as described for the 2-cyclohexylamino derivative (Example 38), an equivalent of n-octylamine replacing the cyclohexylamine. The crude product is purified by recrystallization from aqueous 2-methoxyethanol and then melts at 130°-132° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04065567 |
| 出典データセット | uspto-grants-1977_12 |
| ORD ID | ord-753b35837da44544a0a6e1d524189248 |
| 出典メモ | uspto-grants-1977_12 |