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9,10-Anthracenedicarboxaldehyde → 9,10-Anthracenedicarboxaldehyde, dihydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 9,10-Anthracenedicarboxaldehyde | HCID 81500 | — |
| 反応物 | 2-Hydrazinoimidazoline dihydrochloride | HCID 12221231 | — |
| 溶媒 | 1-Propanol | HCID 1031 | — |
| 生成物 | 9,10-Anthracenedicarboxaldehyde, dihydrochloride | HCID 19762841 | — |
反応手順
A suspension of 5.0 g of 9,10-anthracenedicarboxaldehyde and 7.8 g of 2-hydrazino-2-imidazoline dihydrochloride in 75 ml of n-propanol is refluxed for 2 hours. The mixture is cooled and the solid is collected giving bis(2-imidazolin-2-ylhydrazone) of 9,10-anthracenedicarboxaldehyde, dihydrochloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04515954 |
| 出典データセット | uspto-grants-1985_05 |
| ORD ID | ord-3a2581060dba434faf9facaffd8891e3 |
| 出典メモ | uspto-grants-1985_05 |