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2-Ethylhexylamine → HCID 178438302、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Ethylhexylamine | HCID 7719 | — |
| 反応物 | Allylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic anhydride | HCID 54206110 | — |
| 生成物 | HCID 178438302 | HCID 178438302 | — |
反応手順
The procedure described in Example 3 is repeated, except that 204 g of allyl-bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid anhydride and 129 g of 2-ethylhexylamine are used. 17 g of water are split off at 115° to 160° C. under 4,000 Pa in the course of 4.5 hours. 292.05 g (92.6% of theory) of a fraction of boiling point 160°-164° C. under 10.7 Pa, nD20 1.5038 and η25 0.68 Pa.s are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04515962 |
| 出典データセット | uspto-grants-1985_05 |
| ORD ID | ord-66646a12f77d4dda98649accf3d14af1 |
| 出典メモ | uspto-grants-1985_05 |