関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2-Propanol, 1,3-dichloro-, 2-carbamate | HCID 68516 | — |
| 反応物 | 1,1-Bis(tert-butylperoxy)cyclohexane | HCID 76359 | — |
| 反応物 | 2-Butenedioic acid (2Z)-, 1,4-ditridecyl ester | HCID 6437427 | — |
| 生成物 | 1,3-dichloropropan-2-yl carbamate;ditridecyl (Z)-but-2-enedioate | HCID 131712900 | — |
反応手順
To a 500 ml resin kettle equipped with an overhead stirrer and containing 200 g of Flo Mo 36 C (ethoxylated castor oil) were added 50 g ditridecyl maleate and 6 g 1,1-bis(t-butylperoxy)cyclohexane (available from Witco Chemical Company under the tradename USP-400P). The mixture was then heated to 110° C. for 4 hours under nitrogen to yield a viscous liquid surfactant of the invention (Surfactant No. 54).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US04520140 |
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| 出典データセット | uspto-grants-1985_05 |
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| ORD ID | ord-3414ce7107c148798ef167c89ac2f26c |
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| 出典メモ | uspto-grants-1985_05 |
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